J. Mater. Sci. Technol. ›› 2021, Vol. 77: 223-236.DOI: 10.1016/j.jmst.2020.10.063
• Research Article • Previous Articles Next Articles
Chengqi Suna,b,*(), Yanqing Lic, Kuilong Xud, Baotong Xue
Received:
2020-08-30
Revised:
2020-10-19
Accepted:
2020-10-21
Published:
2021-06-30
Online:
2020-11-20
Contact:
Chengqi Sun
About author:
* State Key Laboratory of Nonlinear Mechanics, Institute of Mechanics, Chinese Academy of Sciences, Beijing, 100190, China. E-mail addresses: scq@lnm.imech.ac.cn (C. Sun).Chengqi Sun, Yanqing Li, Kuilong Xu, Baotong Xu. Effects of intermittent loading time and stress ratio on dwell fatigue behavior of titanium alloy Ti-6Al-4V ELI used in deep-sea submersibles[J]. J. Mater. Sci. Technol., 2021, 77: 223-236.
Fig. 1. Microstructures in the transverse section of specimens. (a) EBSD grain map and (b) EBSD phase map corresponding to (a); α- and β-phase are denoted in green and red, respectively.
Fig. 2. Shapes and dimensions of specimens (in mm) for (a) tensile test, (b) creep test, and (c) conventional fatigue test and dwell fatigue test at stress ratio R = 0.
Fig. 3. Schematics of loading waveforms. (a) Conventional fatigue test performed using continuous triangular wave (dt,min = 0) or intermittent triangular wave (dt,min > 0); (b) Dwell fatigue test performed using continuous trapezoidal wave ( dt,min = 0) or intermittent trapezoidal wave (dt,min> 0).
Maximum stress (MPa) | Dwell timedt ,max (s) | Minimum stress (MPa) | Intermittent loading timedt ,min (s) | Stress ratio,R | Fatigue life (cyc) | Failure mode |
---|---|---|---|---|---|---|
815 | 120 | 0 | 0 | 0 | 2373 | Fatigue |
815 | 120 | 0 | 0 | 0 | 2384 | Mixed |
815 | 120 | 0 | 0 | 0 | 1028 | Mixed |
815 | 120 | 0 | 2 | 0 | 3669 | Ductile |
815 | 120 | 0 | 2 | 0 | 3391 | Fatigue |
815 | 120 | 0 | 2 | 0 | 2099 | Mixed |
815 | 120 | 0 | 12 | 0 | 5096 | Ductile |
815 | 120 | 0 | 12 | 0 | 2198 | Mixed |
815 | 120 | 0 | 12 | 0 | 2456 | Mixed |
815 | 120 | 0 | 60 | 0 | 1844 | Mixed |
815 | 120 | 0 | 60 | 0 | 1714 | Mixed |
815 | 0 | 0 | 0 | 0 | 18,317 | Fatigue |
815 | 0 | 0 | 0 | 0 | 19,585 | Fatigue |
815 | 0 | 0 | 12 | 0 | 15,920 | Fatigue |
815 | 0 | 0 | 12 | 0 | 17,098 | Fatigue |
Table 1. Loading information and associated fatigue life and failure mode data for specimens in Fig. 4.
Maximum stress (MPa) | Dwell timedt ,max (s) | Minimum stress (MPa) | Intermittent loading timedt ,min (s) | Stress ratio,R | Fatigue life (cyc) | Failure mode |
---|---|---|---|---|---|---|
815 | 120 | 0 | 0 | 0 | 2373 | Fatigue |
815 | 120 | 0 | 0 | 0 | 2384 | Mixed |
815 | 120 | 0 | 0 | 0 | 1028 | Mixed |
815 | 120 | 0 | 2 | 0 | 3669 | Ductile |
815 | 120 | 0 | 2 | 0 | 3391 | Fatigue |
815 | 120 | 0 | 2 | 0 | 2099 | Mixed |
815 | 120 | 0 | 12 | 0 | 5096 | Ductile |
815 | 120 | 0 | 12 | 0 | 2198 | Mixed |
815 | 120 | 0 | 12 | 0 | 2456 | Mixed |
815 | 120 | 0 | 60 | 0 | 1844 | Mixed |
815 | 120 | 0 | 60 | 0 | 1714 | Mixed |
815 | 0 | 0 | 0 | 0 | 18,317 | Fatigue |
815 | 0 | 0 | 0 | 0 | 19,585 | Fatigue |
815 | 0 | 0 | 12 | 0 | 15,920 | Fatigue |
815 | 0 | 0 | 12 | 0 | 17,098 | Fatigue |
Fig. 5. Photographs and fracture surface morphologies of failed specimens subjected to dwell fatigue tests at σmax=815 MPa, dt,max = 120 s, σmin=0 MPa, and dt,min = 0 s. A-1 to A-4: Nf = 2373 cycles; A-1 is photograph of fractured specimen, A-2 is SEM image of fracture surface, and A-3 and A-4 are magnified images of regions corresponding to up and down arrows in A-2, respectively. B-1 to B-4: Nf = 2384 cycles, B-1 is photograph of fractured specimen, B-2 is SEM image of fracture surface, and B-3 and B-4 are magnified images of regions corresponding to up and right arrows in B-2, respectively. C-1 to C-4: Nf = 1028 cycles; C-1 is photograph of fractured specimen, C-2 is SEM image of fracture surface, and C-3 and C-4 are magnified images of regions corresponding to lower left and down arrows in C-2, respectively.
Fig. 6. Photographs and fracture surface morphologies of failed specimens subjected to dwell fatigue tests at σmax=815 MPa, dt,max = 120 s, σmin=0 MPa, and dt,min = 2 s. A-1 to A-4: Nf = 3391 cycles, A-1 is photograph of fractured specimen, A-2 is SEM image of fracture surface, and A-3 and A-4 are magnified images of regions corresponding to arrows in A-2 and A-3, respectively. B-1 to B-4: Nf = 3669 cycles, B-1 is photograph of fractured specimen, B-2 is SEM image of fracture surface, and B-3 and B-4 are magnified images of regions corresponding to up and right arrows in B-2, respectively. C-1 to C-4: Nf = 2099 cycles; C-1 is photograph of fractured specimen, C-2 is SEM image of fracture surface, and C-3 and C-4 are magnified images of regions corresponding to left and down arrows in C-2, respectively.
Fig. 7. Photographs and fracture surface morphologies of failed specimens subjected to dwell fatigue test and tensile test. A-1 to A-4, B-1 to B-4, and C-1 to C-4: specimens subjected to dwell fatigue test, σmax=815 MPa, dt,max = 120 s, σmin=0 MPa, and dt,min = 12 s. A-1 to A-4: Nf = 2198 cycles; A-1 is photograph of fractured specimen, A-2 is SEM image of fracture surface, and A-3 and A-4 are magnified images of regions corresponding to arrows in A-2 and A-3, respectively; B-1 to B-4: Nf = 5096 cycles; B-1 is photograph of fractured specimen, B-2 is SEM picture of fracture surface, and B-3 and B-4 are magnified images of regions corresponding to up and down arrows in B-2, respectively. C-1 to C-4: Nf = 2456 cycles, C-1 is photograph of fractured specimen, C-2 is SEM image of fracture surface, and C-3 and C-4 are magnified images of regions corresponding to left and down arrows in C-2, respectively. d-1 to d-4: tensile specimen, d-1 is SEM image of fracture surface, d-2 is SEM image of fracture surface, and d-3 and d-4 are magnified images of regions corresponding to arrows in d-2 and d-3, respectively.
Fig. 8. Photographs and fracture surface morphologies of failed specimens subjected to dwell fatigue tests at σmax=815 MPa, dt,max = 120 s, σmin=0 MPa, and dt,min = 60 s. A-1 to A-4: Nf = 1844 cycles; A-1 is photograph of fracture specimen, A-2 is SEM image of fracture surface, and A-3 and A-4 are magnified images of regions corresponding to arrows in A-2 and A-3, respectively. B-1 to B-4: Nf = 1714 cycles; B-1 is photograph of fractured specimen, B-2 is SEM image of fracture surface, and B-3 and B-4 are magnified images of regions corresponding to left and down arrows in B-2, respectively.
Fig. 9. Fracture surface morphologies of failed specimens subjected to conventional fatigue test and intermittent conventional fatigue test. A-1 to A-3 and B-1 to B-3: specimens subjected to conventional fatigue test, σmax=815 MPa and σmin=0 MPa. A-1 to A-3: Nf = 18,317 cycles; A-1 is SEM image of fracture surface, and A-2 and A-3 are magnified images of regions corresponding to up and down arrows in A-1, respectively; B-1 to B-3: Nf = 19,585 cycles; B-1 is SEM image of fracture surface, and B-2 and B-3 are magnified images of regions corresponding to arrows in B-1 and B-2, respectively. C-1 to C-3 and d-1 to d-3: Specimens subjected to intermittent conventional fatigue test, σmax=815 MPa, σmin=0 MPa, and dt,min = 12 s; C-1 to C-3: Nf = 15,920 cycles; C-1 is SEM image of fracture surface, and C-2 and C-3 are magnified images of regions corresponding to right and lower-right arrows in C-1, respectively; d-1 to d-3: Nf = 17,098 cycles; d-1 is SEM image of fracture surface, and d-2 and d-3 are magnified images of regions corresponding to left and right arrows in d-1, respectively.
Fig. 10. Variations in cumulative maximum strain (εmax) and minimum strain (εmin) with number of loading cycles for specimens fractured within extensometer during dwell fatigue tests performed at σmax=815 MPa, σmin=0 MPa, and dt,max = 120 s.
Fig. 11. Dwell fatigue life at different stress ratios R. Lines denote linear regression results. (a) Fatigue life versus R and (b) fatigue life versus (1-R)/2.
Maximum stress (MPa) | Dwell timedt ,max (s) | Minimum stress (MPa) | Intermittent loading timedt ,min (s) | Stress ratioR | Fatigue life (cyc) |
---|---|---|---|---|---|
815 | 120 | -815 | 0 | -1 | 207 |
815 | 120 | -815 | 0 | -1 | 269 |
815 | 120 | -407.5 | 0 | -0.5 | 761 |
Table 2. Loading information and associated fatigue life data for negative stress ratios shown in Fig. 11.
Maximum stress (MPa) | Dwell timedt ,max (s) | Minimum stress (MPa) | Intermittent loading timedt ,min (s) | Stress ratioR | Fatigue life (cyc) |
---|---|---|---|---|---|
815 | 120 | -815 | 0 | -1 | 207 |
815 | 120 | -815 | 0 | -1 | 269 |
815 | 120 | -407.5 | 0 | -0.5 | 761 |
Fig. 12. Photographs and fracture surface morphologies of failed specimens subjected to dwell fatigue tests at negative stress ratios. A-1 to A-4: σmax=815 MPa, dt,max = 120 s, σmin=-815 MPa, dt,min = 0 s, and Nf = 207 cycles; A-1 is photograph of fractured specimen, A-2 is SEM image of fracture surface, and A-3 and A-4 are magnified images of regions corresponding to down and up arrows in A-2, respectively. B-1 to B-4: σmax=815 MPa, dt,max = 120 s, σmin=-815 MPa, dt,min = 0 s, and Nf = 269 cycles; B-1 is photograph of fractured specimen, B-2 is SEM image of fracture surface, and B-3 and B-4 are magnified images of regions corresponding to down and up arrows in B-2, respectively; C-1 to C-4: σmax=815 MPa, dt,max = 120 s, σmin=-407.5 MPa, dt,min = 0 s, and Nf = 761 cycles, C-1 is photograph of fractured specimen, C-2 is SEM image of fracture surface, and C-3 and C-4 are magnified images of regions corresponding to down and up arrows in C-2, respectively.
Fig. 13. Variations in cumulative maximum strain (εmax) and minimum strain (εmin) with number of loading cycles for dwell-fatigued specimens fractured within extensometer at σmax=815 MPa, dt,max = 120 s, and dt,min = 0 and different stress ratios.
Fig. 14. Effects of prior creep and fatigue loading on tensile behavior. Prior-creep stress is 815 MPa and fatigue loading is σmax=815 MPa, dt,max = 0 s, σmin = 0, and dt,min = 0.
Loading type | Tensile strength (MPa) | Yield strength (MPa) |
---|---|---|
Tensile | 930 | 855 |
Tensile | 929 | 846 |
Tensile | 940 | 857 |
Creep for 100 h then tensile | 950 | 945 |
Creep for 200 h then tensile | 959 | 956 |
500 cycles then tensile | 917 | 860 |
Table 3. Tensile strength and yield strength for specimens after being subjected to prior creep or fatigue loading.
Loading type | Tensile strength (MPa) | Yield strength (MPa) |
---|---|---|
Tensile | 930 | 855 |
Tensile | 929 | 846 |
Tensile | 940 | 857 |
Creep for 100 h then tensile | 950 | 945 |
Creep for 200 h then tensile | 959 | 956 |
500 cycles then tensile | 917 | 860 |
Fig. 15. Effect of prior creep on conventional fatigue life, diameter of test section of specimens, and cumulative strain as function of number of loading cycles. (a) Fatigue life versus prior creep time; prior-creep stress is 815 MPa as calculated based on initial diameter of test section of specimens, subsequent fatigue loading is σmax=815 MPa, dt,max = 0 s, σmin = 0, dt,min = 0, and maximum stress for fatigue loading was calculated based on initial diameter of test section of specimens. (b) Ratio of diameter of test section of specimens after prior creep to that before prior creep in (a). (c) Maximum stress versus fatigue life. Here, prior-creep stress is 815 MPa as calculated based on initial diameter of test section of specimens, and maximum stress during subsequent fatigue loading was calculated based on diameter of test section of specimens after being subjected to prior-creep. (d) Cumulative maximum strain (εmax) and minimum strain (εmin) versus number of loading cycles for prior-creep specimens fractured within extensometer. Herein, prior-creep stress is 815 MPa as calculated based on initial diameter of test section of specimens, and maximum stress during subsequent fatigue loading is 815 MPa as calculated based on initial diameter of test section of specimens.
Specimen No. | After prior creep for 10 h | Immediately after complete unloading after prior creep for 10 h |
---|---|---|
1 | 3.45% | 2.68 % |
2 | 3.69% | 2.96 % |
3 | 3.83% | 3.08 % |
Table 4. Cumulative strains after prior creep for 10 h and immediately after complete unloading after prior creep for 10 h for specimens subjected to prior creep for 10 h.
Specimen No. | After prior creep for 10 h | Immediately after complete unloading after prior creep for 10 h |
---|---|---|
1 | 3.45% | 2.68 % |
2 | 3.69% | 2.96 % |
3 | 3.83% | 3.08 % |
Fig. 16. Variations in cumulative maximum strain with loading time for specimens fractured within extensometer during dwell fatigue test with σmax=815 MPa and σmin=0 MPa. Results for creep tests are shown for comparison. The stress for creep tests is calculated based on initial diameter of test section of specimens.
Fig. 17. Effects of dwell loading and prior creep on cumulative maximum strain of specimens fractured within extensometer. (a) Cumulative maximum strain versus number of loading cycles, σmax=815 MPa and σmin=0 MPa. Specimens subjected to prior creep for 200 h at σ =815 MPa exhibited plastic strain because of creep and then fatigue. The stress for prior creep is calculated based on initial diameter of test section of the specimen. (b) Cumulative maximum strain versus loading time, σmax=815 MPa and σmin=0 MPa.
Fig. 18. Fatigue life versus cumulative maximum strain (εmax) during first loading cycle of dwell fatigue test. Line denotes linear regression result for dwell fatigue life (Nf) on logarithmic scale and strain (εmax) on logarithmic scale.
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