J. Mater. Sci. Technol. ›› 2024, Vol. 197: 238-246.DOI: 10.1016/j.jmst.2024.01.077

Special Issue: Composites 2024 Modeling, computation, and simulation 2024 Nuclear materials 2024

• Research Article • Previous Articles     Next Articles

The synergetic effect of He and Kr irradiation on helium bubble evolution in SiC/SiC composite: Combining in-situ TEM observation with MD simulation

Shanshan Xua, Ce Zhenga,*, Xiaoqiang Lia,*, Ning Gaob, Zijing Huangc, Jian Zhangc, Chong Weia,d, Cheng Zhanga   

  1. aScience and Technology on Thermo Structural Composite Materials Laboratory, Northwestern Polytechnical University, Xi’an 710072, China;
    bInstitute of Frontier and Interdisciplinary Science and Key Laboratory of Particle Physics and Particle Irradiation (MOE), Shandong University, Qingdao 266237, China;
    cCollege of Energy, Xiamen University, Xiamen 361005, China;
    dSchool of Mechanics, Civil Engineering and Architecture, Northwestern Polytechnical University, Xi’an 710072, China
  • Received:2023-12-09 Revised:2024-01-19 Accepted:2024-01-23 Published:2024-10-20 Online:2024-10-15
  • Contact: *E-mail addresses: cezheng@nwpu.edu.cn (C. Zheng), xiaoqiangli@nwpu.edu.cn (X. Li)

Abstract: SiC fiber reinforced SiC matrix composites (SiC/SiC composites) are considered as one of the promising structural materials for liquid type breeding blanket in the fusion energy system. The transmutation gas production rate in fusion reactor is significantly higher compared with fission reactors. An innovative method combining in-situ irradiation and TEM observation and MD simulation was utilized to evaluate the synergetic effects of helium and irradiation on SiC/SiC composites. A comprehensive experiment matrix including Kr irradiation, He pre-implantation with sequential Kr irradiation as well as simultaneous dual beam at 1073 K to 16 dpa and 2400 appm He (150 appm/dpa) was performed using 800 keV Kr and 50 keV He ions. With the support of MD results, the impact of relative concentration ratio of vacancies and helium atoms on the bubble evolution was systematically investigated and the corresponding mechanism was further unraveled, which provides the basis of limiting the bubble density in SiC/SiC composites. Additionally, the direct evidence for the competition of irradiation-assisted bubble growth and re-dissolution was in-situ observed in SiC matrix for the first time.

Key words: SiC, In-situ, Irradiation, TEM, Bubble, Molecular dynamics simulation