J. Mater. Sci. Technol. ›› 2024, Vol. 174: 157-167.DOI: 10.1016/j.jmst.2023.03.052

• Research Article • Previous Articles     Next Articles

Precipitation transformation pathway and mechanical behavior of nanoprecipitation strengthened Fe-Mn-Al-C-Ni austenitic low-density steel

Y.F. Ana, X.P. Chena,*, L. Meib, P. Rena, D. Weia, W.Q. Caoc,*   

  1. aCollege of Materials Science and Engineering, Chongqing University, Chongqing 400044, China;
    bGuangxi Engineering Research Center for Characteristic Metallic Powder Materials, School of Electronic Engineering, Guangxi University of Science and Technology, Liuzhou 545006, China;
    cCentral Iron & Steel Research Institute, Beijing 100081, China
  • Received:2023-03-05 Revised:2023-03-26 Accepted:2023-03-27 Published:2024-03-01 Online:2023-05-19
  • Contact: *E-mail addresses: xpchen@cqu.edu.cn (X.P. Chen), caowenquan@nercast.com (W.Q. Cao)

Abstract: Precipitation strengthening has been widely adopted in austenitic low-density steel owing to excellent hardened effects. This approach generally employs the coherent κ′-carbides and non-coherent B2 particles. Revealing the precipitation transformation pathway is decisive for further optimizing the microstructures under specific engineering applications. Herein, the detailed precipitation sequence of Fe-28Mn-11Al-1C-5Ni (wt%) austenitic low-density steel as well as its influence on mechanical properties during aging process is systematically investigated. Our results reveal that nano-sized κ′-carbides domains (2 nm) exist in the solution-treated specimen. During aging at 500 °C for 1 h, the cuboidal κ′-carbides (15-20 nm) uniformly disperse in austenite matrix. However, after aging at 700 °C for 15 min, the coarsen κ′-carbides (30-35 nm) inhomogeneously distribute and align preferentially along the 〈1 0 0〉 directions. Further, extending the aging time to 60 min, the needle-type B2 particles replace the κ′-carbides due to the enrichment of Ni elements at the phase boundaries among the austenite and κ′-carbides. After aging at 900 °C, κ′-carbides entirely dissolve into the austenite matrix, and the intragranular B2 particles are the sole precipitates in the austenite matrix and follow the K-S orientation relationship with austenite. The work hardening capability seriously deteriorates due to the shearing of κ′-carbides by gliding dislocations. While the intragranular B2 particles preserve excellent work hardening rate by dislocations bow-out mechanism. The present work is meaningful for guiding the design of new generation dual-nano precipitation austenitic lightweight steel.

Key words: Lightweight steel, κ'-carbides, B2 particles, Work hardening capability