Porosity and Oxide Layer Dependence of Thermal Shock Behavior of Porous Silicon Nitride Ceramics

doi:10.1016/j.jmst.2014.11.004

J. Mater. Sci. Technol. ›› 2014, Vol. 30 ›› Issue (12): 1217-1222.DOI: 10.1016/j.jmst.2014.11.004

• Orginal Article • Previous Articles Next Articles

Porosity and Oxide Layer Dependence of Thermal Shock Behavior of Porous Silicon Nitride Ceramics

Xuefeng Lu¹, Yin Wei¹, Hongjie Wang¹, Jiangbo Wen¹, Jun Zhou², Jinpeng Fan²

1、State Key Laboratory for Mechanical Behavior of Materials, School of Materials Science and Engineering, Xi'an Jiaotong University, Xi'an 710049, China; 2、National Key Laboratory of Advanced Functional Composite Materials, Beijing 100076, China

Revised:2014-08-26 Online:2014-12-20 Published:2015-07-23

Abstract

Abstract: A water-quenching technique has been adopted to evaluate thermal shock fracture and fatigue behaviors of porous Si₃N₄ ceramics in an air atmosphere. The high-porosity Si₃N₄ ceramics exhibit a higher strength retention and a better resistance to thermal shock fatigue because of its role of the pores as crack arresters. A dense and coherent surface oxide layer leads to a significant benefit in residual strength during thermal fatigue, however, an increased fatigue number to 30th cycle cannot cause a further influence although a thicker oxide layer presents, which is attributed to holes defect and disappearance of part intergranular phase.

Key words: Porous silicon nitride ceramics, Oxide layer, Thermal shock behavior, Thermal fatigue

Xuefeng Lu, Yin Wei, Hongjie Wang, Jiangbo Wen, Jun Zhou, Jinpeng Fan. Porosity and Oxide Layer Dependence of Thermal Shock Behavior of Porous Silicon Nitride Ceramics[J]. J. Mater. Sci. Technol., 2014, 30(12): 1217-1222.

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Porosity and Oxide Layer Dependence of Thermal Shock Behavior of Porous Silicon Nitride Ceramics

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