材料科学与技术 ›› 2018, Vol. 34 ›› Issue (12): 2263-2270.DOI: 10.1016/j.jmst.2018.06.010

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  • 收稿日期:2017-05-22 修回日期:2017-08-13 接受日期:2017-09-13 出版日期:2018-12-20 发布日期:2018-11-15

Structural characterization and strengthening mechanism of forsterite nanostructured scaffolds synthesized by multistep sintering method

Fariborz Tavangariana*(), Abbas Fahamib, Guoqiang Lic, Mohammadhassan Kazemid, Anoosha Forghanie   

  1. a Mechanical Engineering Program, School of Science, Engineering and Technology, Pennsylvania State University, Harrisburg, Middletown, PA, 17057, USA
    b Department of Mechanical Engineering, Texas A&M University, College Station, TX 77843-3123, USA;
    c Department of Mechanical and industrial Engineering, Louisiana State University, Baton Rouge, LA, 70803, USA
    d Department of Mechanical and Aerospace Engineering, University at Buffalo, Buffalo, 14260, NY, USA
    e Department of Biomedical Engineering, Millennium Science Complex, Pennsylvania State University, University Park, PA, 16802, USA
  • Received:2017-05-22 Revised:2017-08-13 Accepted:2017-09-13 Online:2018-12-20 Published:2018-11-15
  • Contact: Tavangarian Fariborz

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Abstract:

In this study, highly porous forsterite scaffolds with interconnected porosities were synthesized using multi-step sintering (MSS) method. The starting powder was nanosized forsterite, which was synthesized from talc and magnesium carbonate powders. The phase composition, average particle size and morphology of the produced forsterite powder were characterized by X-ray diffraction technique (XRD) and transition electron microscopy (TEM). Forsterite scaffolds were produced by foamy method using polymeric sponges. MSS process including three steps was used to efficiently sinter the forsterite nanopowders without destroying the initial porous structure of polymeric sponges. The results showed that MSS technique is an efficient and appropriate procedure to produce highly porous forsterite scaffolds with pore size in the range of 100-300?μm. The compressive strength, compressive modulus and porosity of C12 specimen (sintered at 1650?°C for 1?h with subsequent annealing at 1000?°C for 1000?min) was 1.88?MPa, 29.2?MPa, and 72.4%, respectively, which is very close to that of cancellous bone. The approach studied in this research can be developed for other nanostructure ceramics to produce highly porous scaffolds with interconnected porosities for load bearing applications.

Key words: Forsterite, Multi-step sintering, Scaffolds, Porosity