An efficient method to engage oxide ceramics in low-temperature interfacial reactions: Microstructure evolution and kinetics behaviors based on supercooling in a transient liquid phase bonding joint

doi:10.1016/j.jmst.2022.10.094

J. Mater. Sci. Technol. ›› 2023, Vol. 151: 234-244.DOI: 10.1016/j.jmst.2022.10.094

• Research Article • Previous Articles Next Articles

An efficient method to engage oxide ceramics in low-temperature interfacial reactions: Microstructure evolution and kinetics behaviors based on supercooling in a transient liquid phase bonding joint

Jia Yang^a,1, Wanqi Zhao^a,b,1, Panpan Lin^a,*, Qiuguang Zhang^a, Xinfei Zhang^a, Tiesong Lin^a,*, Peng He^a,*, Yanli Zhuang^c

^aState Key Laboratory of Advanced Welding and Joining, Harbin Institute of Technology, Harbin 150001, China;
^bAECC Shenyang Liming Aero-Engine Co., Ltd, Shenyang 110043, China;
^cHeilongjiang Provincial Key Laboratory of CO2 Resource Utilization and Energy Catalytic Materials, School of Material Science and Chemical Engineering, Harbin University of Science and Technology, Harbin 150040, China

Received:2022-07-24 Revised:2022-10-17 Accepted:2022-10-28 Published:2023-07-10 Online:2023-02-05
Contact: * E-mail addresses: pplin@hit.edu.cn (P. Lin), hitjoining@hit.edu.cn (T. Lin), hithepeng@hit.edu.cn (P. He).
About author:¹ These authors contributed equally to this work.

Abstract

Abstract: Ductile transient liquid phase (TLP) bonding joints reinforced by multiple precipitates were produced using novel pre-sintered coatings and Au-Si fillers; therefore, the highest strength of NiTi/sapphire joints brazed at 460 °C for 30 min reached 72 MPa. The pre-sintering process improved the surface-active of sapphire by forming metastable Ti₃O and non-stoichiometric Al₂O₃. The typical brazing seam consisted of O-rich compounds, TiSi₂, and Ti-Ni-Si, wherein the O-rich phase featured different crystallinity depending on the oxygen content. The sapphire/seam interface was either a nanoscale diffusion region or a Si-rich amorphous layer. The breakdown of the Stokes-Einstein relation (SER) occurred, and the deviation from SER increased with a higher cooling rate. The influence of coating thickness was reflected in (i) the supercooling related to the viscosity and fractional exponent of liquids and (ii) the microstructural change of the joint related to the driving force for crystal growth. This work presented a new strategy for joining ceramics to metals at lower temperatures but using the joint at higher temperatures; furthermore, gave an insight into the microstructure evolution and kinetics behaviors based on supercooling in a transient liquid phase bonding joint.

Key words: Sapphire, NiTi, Reinforced ductile fillers, Transient liquid phase bonding, Surface modification, Kinetic behaviors

Jia Yang, Wanqi Zhao, Panpan Lin, Qiuguang Zhang, Xinfei Zhang, Tiesong Lin, Peng He, Yanli Zhuang. An efficient method to engage oxide ceramics in low-temperature interfacial reactions: Microstructure evolution and kinetics behaviors based on supercooling in a transient liquid phase bonding joint[J]. J. Mater. Sci. Technol., 2023, 151: 234-244.

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An efficient method to engage oxide ceramics in low-temperature interfacial reactions: Microstructure evolution and kinetics behaviors based on supercooling in a transient liquid phase bonding joint

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