J. Mater. Sci. Technol. ›› 2023, Vol. 134: 178-188.DOI: 10.1016/j.jmst.2022.05.060
• Research Article • Previous Articles Next Articles
S.P. Zhaoa, Z.D. Fenga, L.X. Lia, X.J. Zhaob, L. Lub, S. Chena, N.B. Zhanga,b,*(), Y. Caia,*(), S.N. Luob
Received:
2022-04-28
Revised:
2022-05-17
Accepted:
2022-05-18
Published:
2023-01-20
Online:
2023-01-10
Contact:
N.B. Zhang,Y. Cai
About author:
caiy@pims.ac.cn (Y. Cai).S.P. Zhao, Z.D. Feng, L.X. Li, X.J. Zhao, L. Lu, S. Chen, N.B. Zhang, Y. Cai, S.N. Luo. Dynamic mechanical properties, deformation and damage mechanisms of eutectic high-entropy alloy AlCoCrFeNi2.1 under plate impact[J]. J. Mater. Sci. Technol., 2023, 134: 178-188.
Fig. 1. Schematic setups for (a) Hugoniot equation of state experiments, (b) shock compression and recovery experiments, and (c) spallation and recovery experiments. 1: polycarbonate sabot; 2: flyer plate; 3: magnetic induction velocimeter; 4: driver plate; 5: AlCoCrFeNi2.1 EHEA sample; 6: sample holder; 7: optical fiber connected to a laser Doppler velocimeter (LDV); 8: recess for release waves; 9: momentum trap ring; 10: momentum trap plate; 11: soft materials; 12: thin turning mirror; 13: lens.
Type | Flyer plate | Driver plate | Sample | Momentum trap plate | ||||
---|---|---|---|---|---|---|---|---|
Empty Cell | d (mm) | h (mm) | d (mm) | h (mm) | d (mm) | h (mm) | d (mm) | h (mm) |
Hugoniot EOS (low velocity) | 26.7 | 2.0 | 22.1 | 2.0 | 13.1 | 3.0 | - | - |
Hugoniot EOS (high velocity) | 18.9 | 2.0 | 22.1 | 2.0 | 13.1 | 3.0 | - | - |
Shock compression | 13.3 | 2.0 | - | - | 10.0 | 1.0 | 10.0 | 3.0 |
Spallation | 13.3 | 1.0 | - | - | 10.0 | 2.0 | - | - |
Table 1. Summary of the diameters and thicknesses of different plates in all three kinds of experiments, d: diameter, h: thickness.
Type | Flyer plate | Driver plate | Sample | Momentum trap plate | ||||
---|---|---|---|---|---|---|---|---|
Empty Cell | d (mm) | h (mm) | d (mm) | h (mm) | d (mm) | h (mm) | d (mm) | h (mm) |
Hugoniot EOS (low velocity) | 26.7 | 2.0 | 22.1 | 2.0 | 13.1 | 3.0 | - | - |
Hugoniot EOS (high velocity) | 18.9 | 2.0 | 22.1 | 2.0 | 13.1 | 3.0 | - | - |
Shock compression | 13.3 | 2.0 | - | - | 10.0 | 1.0 | 10.0 | 3.0 |
Spallation | 13.3 | 1.0 | - | - | 10.0 | 2.0 | - | - |
Fig. 2. TEM characterization of the as-cast AlCoCrFeNi2.1 EHEA. (a) Bright-field image of the lamellar structure. (b) and (c) Selected area electron diffraction (SAED) patterns corresponding to the L12 and B2 phases, respectively. Super-lattice diffraction spots are indicated by the blue and red circles, respectively. ZA: zone axis.
Fig. 3. EBSD characterization of the as-cast AlCoCrFeNi2.1 EHEA. (a) Phase map. (b) Phase map and (c) corresponding inverse pole figure map of two adjacent grains, grain-1 and grain-2. (d) {110} and {111} pole figures of the intragranular BCC domains and parent FCC domains for grain-1 and grain-2.
Shot No. | ds (mm) | uimp (km s−1) | up1 (km s−1) | us1 (km s−1) | σHEL (GPa) | up2 (km s−1) | us2 (km s−1) | σH (GPa) |
---|---|---|---|---|---|---|---|---|
EOS-1 | 3.049(2) | 0.321(1) | 0.017(1) | 6.126(8) | 0.777(9) | 0.159(1) | 5.019(9) | 6.022(13) |
EOS-2 | 3.038(2) | 0.454(1) | 0.017(1) | 6.097(8) | 0.757(9) | 0.227(1) | 5.128(10) | 8.684(18) |
EOS-3 | 3.039(2) | 0.503(1) | 0.018(1) | 6.115(8) | 0.814(9) | 0.251(1) | 5.149(10) | 9.660(21) |
EOS-4 | 3.045(2) | 0.616(1) | 0.011(1) | 6.018(8) | 0.466(6) | 0.309(1) | 5.244(10) | 12.011(25) |
EOS-5 | 3.045(2) | 0.717(1) | 0.023(1) | 5.994(8) | 1.003(12) | 0.361(1) | 5.279(10) | 14.177(30) |
EOS-6 | 3.049(2) | 0.846(1) | 0.024(1) | 6.069(8) | 1.060(12) | 0.426(1) | 5.411(11) | 17.090(35) |
EOS-7 | 3.043(2) | 0.970(1) | 0.020(1) | 5.989(8) | 0.870(10) | 0.491(1) | 5.477(11) | 19.873(41) |
EOS-8 | 3.053(2) | 1.247(2) | 0.021(1) | 6.013(8) | 0.927(11) | 0.635(1) | 5.660(12) | 26.514(55) |
EOS-9 | 3.038(2) | 1.487(2) | 0.028(1) | 6.103(8) | 1.278(15) | 0.755(1) | 5.904(13) | 32.864(68) |
Table 2. Summary of experimental parameters and results for the Hugoniot equation of state experiments. ds: sample thickness; uimp: impact velocity; up1: elastic shock particle velocity; us1: elastic shock wave velocity; σHEL: the Hugoniot elastic limit stress; up2: plastic shock particle velocity; us2: plastic shock wave velocity; σH: peak shock stress. Numbers in parentheses denote uncertainties in the last 1 or 2 digits.
Shot No. | ds (mm) | uimp (km s−1) | up1 (km s−1) | us1 (km s−1) | σHEL (GPa) | up2 (km s−1) | us2 (km s−1) | σH (GPa) |
---|---|---|---|---|---|---|---|---|
EOS-1 | 3.049(2) | 0.321(1) | 0.017(1) | 6.126(8) | 0.777(9) | 0.159(1) | 5.019(9) | 6.022(13) |
EOS-2 | 3.038(2) | 0.454(1) | 0.017(1) | 6.097(8) | 0.757(9) | 0.227(1) | 5.128(10) | 8.684(18) |
EOS-3 | 3.039(2) | 0.503(1) | 0.018(1) | 6.115(8) | 0.814(9) | 0.251(1) | 5.149(10) | 9.660(21) |
EOS-4 | 3.045(2) | 0.616(1) | 0.011(1) | 6.018(8) | 0.466(6) | 0.309(1) | 5.244(10) | 12.011(25) |
EOS-5 | 3.045(2) | 0.717(1) | 0.023(1) | 5.994(8) | 1.003(12) | 0.361(1) | 5.279(10) | 14.177(30) |
EOS-6 | 3.049(2) | 0.846(1) | 0.024(1) | 6.069(8) | 1.060(12) | 0.426(1) | 5.411(11) | 17.090(35) |
EOS-7 | 3.043(2) | 0.970(1) | 0.020(1) | 5.989(8) | 0.870(10) | 0.491(1) | 5.477(11) | 19.873(41) |
EOS-8 | 3.053(2) | 1.247(2) | 0.021(1) | 6.013(8) | 0.927(11) | 0.635(1) | 5.660(12) | 26.514(55) |
EOS-9 | 3.038(2) | 1.487(2) | 0.028(1) | 6.103(8) | 1.278(15) | 0.755(1) | 5.904(13) | 32.864(68) |
Fig. 6. Free-surface velocity histories, ufs(t), for the spallation-recovery experiments. Numbers on the curves denote impact velocities uimp in m s?1.
Shot No. | df (mm) | ds (mm) | uimp (m s−1) | σH (GPa) | ∆ufs (m s−1) | σsp (GPa) | ar (108 m s−2) | |
---|---|---|---|---|---|---|---|---|
SP-1 | 1.020 | 1.985 | 200 | 3.80 | 0.757 | - | - | - |
SP-2 | 1.008 | 2.003 | 227 | 4.30 | 0.911 | 153.65 | 3.00 | 3.80 |
SP-3 | 0.987 | 1.940 | 302 | 5.73 | 1.256 | 164.71 | 3.21 | 5.68 |
SP-4 | 1.012 | 2.003 | 410 | 7.81 | 1.377 | 166.31 | 3.24 | 7.13 |
SP-5 | 1.008 | 1.996 | 504 | 9.70 | 1.644 | 171.66 | 3.35 | 8.10 |
SP-6 | 1.005 | 1.937 | 620 | 12.06 | 1.782 | 176.07 | 3.43 | 10.47 |
SP-7 | 1.001 | 2.000 | 730 | 14.40 | 2.037 | 186.74 | 3.64 | 11.69 |
SP-8 | 0.999 | 1.995 | 862 | 17.26 | 2.072 | 187.30 | 3.65 | 12.81 |
SC-1 | 1.012 | 3.023 | 317 | 6.08 | - | - | - | - |
SC-2 | 1.012 | 3.023 | 624 | 12.22 | - | - | - | - |
Table 3. Summary of experimental parameters and results for spallation (SP) and shock compression (SC) recovery experiments. df: flyer thickness; ds: sample thickness; uimp: impact velocity; σH: peak shock stress; $\dot{\varepsilon}$: tensile strain rate; ?ufs: pullback velocity; σsp: spall strength; ar: re-acceleration.
Shot No. | df (mm) | ds (mm) | uimp (m s−1) | σH (GPa) | ∆ufs (m s−1) | σsp (GPa) | ar (108 m s−2) | |
---|---|---|---|---|---|---|---|---|
SP-1 | 1.020 | 1.985 | 200 | 3.80 | 0.757 | - | - | - |
SP-2 | 1.008 | 2.003 | 227 | 4.30 | 0.911 | 153.65 | 3.00 | 3.80 |
SP-3 | 0.987 | 1.940 | 302 | 5.73 | 1.256 | 164.71 | 3.21 | 5.68 |
SP-4 | 1.012 | 2.003 | 410 | 7.81 | 1.377 | 166.31 | 3.24 | 7.13 |
SP-5 | 1.008 | 1.996 | 504 | 9.70 | 1.644 | 171.66 | 3.35 | 8.10 |
SP-6 | 1.005 | 1.937 | 620 | 12.06 | 1.782 | 176.07 | 3.43 | 10.47 |
SP-7 | 1.001 | 2.000 | 730 | 14.40 | 2.037 | 186.74 | 3.64 | 11.69 |
SP-8 | 0.999 | 1.995 | 862 | 17.26 | 2.072 | 187.30 | 3.65 | 12.81 |
SC-1 | 1.012 | 3.023 | 317 | 6.08 | - | - | - | - |
SC-2 | 1.012 | 3.023 | 624 | 12.22 | - | - | - | - |
Fig. 7. Spall strength versus peak shock stress for AlCoCrFeNi2.1 (this work), Al0.1CoCrFeNi (Ref. [45]), FeCrMnNi (Ref. [43]), hot-rolling quenched Fe50Mn30Co10Cr10 (HRQ, Ref. [41]), and cold-rolling quenched Fe50Mn30Co10Cr10 (CRQ, Ref. [41]).
Fig. 8. EBSD characterizations of the impact surface for shots SC-1 (the top row) and SC-2 (the bottom row). (a) and (c) Phase maps, (b) and (d) corresponding KAM maps, and (e) KAM statistics of the FCC (L12) and BCC (B2) phases.
Fig. 9. TEM characterizations of the postmortem samples from (a-f) shot SC-1 and (g-l) shot SC-2. Super-lattice diffraction spots in SAED patterns are indicated by the blue or red circles.
Fig. 10. HRTEM characterization of shot SC-1. (a) Nanotwin and (b) stacking faults (SFs) in the FCC (L12) phase. (c) HRTEM image for the BCC (B2) phase. Two Fourier transformation patterns are also shown.
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