J. Mater. Sci. Technol. ›› 2022, Vol. 106: 225-235.DOI: 10.1016/j.jmst.2021.09.001
• Research Article • Previous Articles Next Articles
Devashish Rajpoota,b, R. Lakshmi Narayanc,*(), Long Zhangd,*(), Punit Kumarb, Haifeng Zhangd, Parag Tandaiyaa, Upadrasta Ramamurtyb,e
Received:
2021-07-28
Revised:
2021-09-01
Accepted:
2021-09-03
Published:
2022-04-20
Online:
2021-10-06
Contact:
R. Lakshmi Narayan,Long Zhang
About author:
zhanglong@imr.ac.cn (L. Zhang).Devashish Rajpoot, R. Lakshmi Narayan, Long Zhang, Punit Kumar, Haifeng Zhang, Parag Tandaiya, Upadrasta Ramamurty. Fracture toughness of a rejuvenated β-Ti reinforced bulk metallic glass matrix composite[J]. J. Mater. Sci. Technol., 2022, 106: 225-235.
Fig. 1. Representative microstructures of (a) as-cast ingot and (b) as-cast bar specimens. Composition line scans of these specimens are shown in (c) and (d), respectively.
Fig. 4. (a) DSC plots obtained on bar and ingot specimens in the as-cast and cryothermal cycling (CTC) states. (b) Variation in enthalpy of relaxation, ΔHrel, with the number of CTC cycles, NCT.
Fig. 5. (a) Representative indentation load-displacement (P-h) response measured on the matrix phase of a composite. (b) Cumulative probability distribution of maximum shear stress, τmax, obtained on the bar and ingot specimens in the as-cast and CTC states.
Material stock | Condition | Mean of first pop-in stress, | Standard deviation of first pop-in stress (GPa) | Coefficient of variation, CV | Number of pop-ins, Npop-in |
---|---|---|---|---|---|
Bar | As-cast | 3.7 | 0.81 | 0.22 | 13 ± 3 |
Ingot | As-cast | 1.79 | 0.46 | 0.26 | 3 ± 1 |
Ingot | CTC (5 cycles) | 1.6 | 0.53 | 0.33 | 6 ± 2 |
Ingot | CTC (10 cycles) | 2.35 | 0.41 | 0.17 | 9 ± 2 |
Ingot | CTC (20 cycles) | 2.22 | 0.35 | 0.16 | 11 ± 1 |
Ingot | CTC (30 cycles) | 2.68 | 0.94 | 0.35 | 11 ± 1 |
Ingot | CTC (60 cycles) | 2.1 | 0.24 | 0.11 | 4 ± 1 |
Table 1. Summary of mechanical properties of as-cast and CTC treated BMGC specimens.
Material stock | Condition | Mean of first pop-in stress, | Standard deviation of first pop-in stress (GPa) | Coefficient of variation, CV | Number of pop-ins, Npop-in |
---|---|---|---|---|---|
Bar | As-cast | 3.7 | 0.81 | 0.22 | 13 ± 3 |
Ingot | As-cast | 1.79 | 0.46 | 0.26 | 3 ± 1 |
Ingot | CTC (5 cycles) | 1.6 | 0.53 | 0.33 | 6 ± 2 |
Ingot | CTC (10 cycles) | 2.35 | 0.41 | 0.17 | 9 ± 2 |
Ingot | CTC (20 cycles) | 2.22 | 0.35 | 0.16 | 11 ± 1 |
Ingot | CTC (30 cycles) | 2.68 | 0.94 | 0.35 | 11 ± 1 |
Ingot | CTC (60 cycles) | 2.1 | 0.24 | 0.11 | 4 ± 1 |
Fig. 6. (a) Representative microstructure of the ingot specimen that was cryothermal cycled (CTC) 30 times. (b) Compositional line and (c) XRD scans obtained across it. (d) Compressive σ-ε responses of the as-cast bar and ingot specimens, and the CTC-30 ingot specimen.
Fig. 7. Microstructures of the compression-tested (a) as-cast bar, (b) as-cast ingot, and (c) CTC-30 ingot specimens. Insets in (a), (b), and (c) are low magnification SEM images of the respective specimens.
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