Mixed-dimensional hierarchical configuration of 2D Ni2P nanosheets anchored on 1D silk-derived carbon fiber for extraordinary electromagnetic wave absorption

doi:10.1016/j.jmst.2021.05.066

Abstract

Abstract:

Considering a series of electromagnetic pollution problems brought by the development of electronic communication technology, more attention has been paid to the research of electromagnetic wave (EMW) absorbing materials with unique composition and structure. Herein, under the inspiration of mixed-dimensional hierarchical structure, 2D Ni₂P nanosheets anchored on 1D silk-derived carbon fiber is successfully fabricated as a gratifying resistor-dielectric type absorber. By a controllable pyrolyzation strategy and disproportionated reaction, high-density 2D Ni₂P nanosheets were grown vertically and cross-linked on the surface of 1D silk-derived carbon fiber. The sample exhibited superior EMW absorption performance with maximum reflection loss value of - 56.9 dB at the thickness of 2.32 mm and the effective absorption bandwidth can reach to 7.2 GHz at the thickness of 1.93 mm. In addition, the pure Ni₂P shows remarkable dielectric characteristic and EMW absorption ability as well. The integration of dual-conductive loss, enhanced polarization relaxation loss and the multiple scattering in the composites was proved to contribute to the good EMW absorption performance. Therefore, this work confirms the great potentials of Ni₂P as a high-efficient EMW absorbing materials and light a new way in construction of multidimensional absorber.

Key words: Biomass, Metal phosphates, Mixed-dimensional hierarchical structure, Impedance match, Electromagnetic wave absorption

Fei Pan, Lei Cai, Yanyan Dong, Xiaojie Zhu, Yuyang Shi, Wei Lu. Mixed-dimensional hierarchical configuration of 2D Ni₂P nanosheets anchored on 1D silk-derived carbon fiber for extraordinary electromagnetic wave absorption[J]. J. Mater. Sci. Technol., 2022, 101: 85-94.

Figures/Tables 10

Fig. 1. The schematic illustration of the NPSCF formation process.

Fig. 2. (a) XRD patterns, (b) FT-IR spectra and (c) Raman spectroscopy of samples.

Fig. 3. SEM images of (a) SCF-700, (b) NOSCF-700 and (c, d, e) NPSCF-700; (f) EDS of P, Ni, and C elements of NPSCF-700.

Fig. 4. (a) XPS survey scan spectra. XPS core-level spectra of (b) C 1s, (c) p 2p and (d) Ni 2p of the NPSCF-700.

Fig. 5. (a, b) Real and imaginary parts of permittivity and (c) dielectric loss tangents.

Fig. 6. Cole-Cole curves of samples: (a) SCF-700, (b) NPSCF-600, (c) NPSCF-700, (d) NPSCF-800.

Fig. 7. Three-dimensional reflection loss mapping, the corresponding contour plots and EMW absorbing properties of samples: (a-c) SCF-700, (d-f) NPSCF-600, (g-i) NPSCF-700, (j-l) NPSCF-800.

Fig. 8. EMW absorption performance of carbon fiber-based materials.

Fig. 9. Calculated delta value maps of samples: (a) SCF-700, (b) NPSCF-600, (c) NPSCF-700, (d) NPSCF-800.

Fig. 10. Schematic illustration of the EMW mechanism in the NPSCF-700.

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Mixed-dimensional hierarchical configuration of 2D Ni₂P nanosheets anchored on 1D silk-derived carbon fiber for extraordinary electromagnetic wave absorption

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