J. Mater. Sci. Technol. ›› 2021, Vol. 73: 76-82.DOI: 10.1016/j.jmst.2020.09.022
• Research Article • Previous Articles Next Articles
Kai Liua,b,c, Hai Zenga,b, Ji Qid,e, Xiaohua Luoa, Xuanwei Zhaoa,b, Xianming Zhenga,b, Yuan Yuana,b, Changcai Chena, Shengcan Maa,*(), Ren Xief, Bing Lid,e, Zhenchen Zhonga
Received:
2020-07-16
Revised:
2020-09-05
Accepted:
2020-09-19
Published:
2021-05-20
Online:
2020-10-03
Contact:
Shengcan Ma
About author:
*E-mail address: mashengcan@jxust.edu.cn (S. Ma).Kai Liu, Hai Zeng, Ji Qi, Xiaohua Luo, Xuanwei Zhao, Xianming Zheng, Yuan Yuan, Changcai Chen, Shengcan Ma, Ren Xie, Bing Li, Zhenchen Zhong. Microstructure and giant baro-caloric effect induced by low pressure in Heusler Co51Fe1V33Ga15 alloy undergoing martensitic transformation[J]. J. Mater. Sci. Technol., 2021, 73: 76-82.
Fig. 1. (a) Heating and cooling DSC curves with the ramp rate of 10 K min-1, (b) Fe-content (x) dependence of martensitic transformation characteristic temperatures ($T_{\text{s}}^{A}$, $T_{\text{f}}^{A}$, $T_{\text{s}}^{M}$ and $T_{\text{f}}^{M}$), (c) Heating and cooling M(T) curves under the applied field of μ0H = 0.1 T, and (d) Magnetization difference (ΔM) across the MT as a function of Fe-content for Co52-xFexV33Ga15 (x = 1, 2, 3, 4) alloys. M(T) curves upon heating and cooling for x = 1 sample and the definition of ΔM are illustrated in the inset of (d).
Fe (x) | 1 | 2 | 3 | 4 |
---|---|---|---|---|
ΔH (J g-1) | 12.9 | 14.6 | 13.2 | 10.5 |
T0 (K) | 320 | 289 | 267 | 236 |
ΔSt (J kg-1 K-1) | 40.3 | 50.5 | 49.4 | 44.5 |
Table 1 The ΔH (J g-1), T0 (K) and ΔSt (J kg-1 K-1) for Co52-xFexV33Ga15 (x = 1, 2, 3, 4) alloys obtained from the DSC data measured with the ramp rate of 10 K min-1.
Fe (x) | 1 | 2 | 3 | 4 |
---|---|---|---|---|
ΔH (J g-1) | 12.9 | 14.6 | 13.2 | 10.5 |
T0 (K) | 320 | 289 | 267 | 236 |
ΔSt (J kg-1 K-1) | 40.3 | 50.5 | 49.4 | 44.5 |
Fig. 2. (a) The microstructure for Co51Fe1V33Ga15 alloy measured by FESEM at room temperature. (b) The distribution results of particle size for V-rich phase. The average particle size is ~1.1 μm obtained by averaging the values of 100 particles.
Fig. 3. Typical BFTEM (a, b) and high-resolution TEM (c, d) images for Co51Fe1V33Ga15 alloy. The SAED images shown in the insets of (a, b) are obtained from the corresponding region in circle, which are in conformity with the respective L21-type and D022-type structures in Co51Fe1V33Ga15 alloy. The other twin variant is denoted by subscript “t”. (e) The FFT result for the region in red box as illustrated in (c). (f) The microstructure of V-rich phase.
Fig. 4. The specific heat capacity as a function of temperature for Co51Fe1V33Ga15 alloy. The value of Cp is from the baseline at T0 = 320 K (the intersection of two blue lines), as illustrated in the black circle.
Fig. 5. Temperature dependence of heat flow curves with the ramp rate of 2 K min-1 (a), total entropy referenced to 330 K (b), isothermal entropy changes (c), and adiabatic temperature changes (d) as a function of temperature for selected hydrostatic pressure upon cooling for Co51Fe1V33Ga15 alloy. The maximum isothermal entropy and adiabatic temperature changes as a function of pressure change are shown in (c) and (d), respectively. (For interpretation of the references to color in this figure legend, the reader is referred to the web version of this article.).
Fig. 6. The maximum adiabatic temperature and isothermal entropy changes normalized to a unit of hydrostatic pressure for state-of-the-art FOMPT alloys with BCE. The data are extracted from Refs. 8, 20, 21, 25-27, 29, and 37.
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