J. Mater. Sci. Technol. ›› 2021, Vol. 67: 165-173.DOI: 10.1016/j.jmst.2020.05.071
• Research article • Previous Articles Next Articles
Xirui Lva,b, Mengkun Yuec,d, Wenfan Yanga,b, Xue Fengc,d, Xiaoyan Lic,d, Yumin Wange, Jiemin Wanga, Jie Zhanga,*(), Jingyang Wanga,*()
Received:
2020-03-13
Revised:
2020-05-21
Accepted:
2020-05-24
Published:
2021-03-20
Online:
2021-04-15
Contact:
Jie Zhang,Jingyang Wang
About author:
jywang@imr.ac.cn (J. Wang).Xirui Lv, Mengkun Yue, Wenfan Yang, Xue Feng, Xiaoyan Li, Yumin Wang, Jiemin Wang, Jie Zhang, Jingyang Wang. Tunable strength of SiCf/β-Yb2Si2O7 interface for different requirements in SiCf/SiC CMC: Inspiration from model composite investigation[J]. J. Mater. Sci. Technol., 2021, 67: 165-173.
Model composites | Sintering temperature (°C) | Density | |
---|---|---|---|
Abs (g/cm3) | Rel (%) | ||
MC1 | 1200 | 5.4 | 88 |
MC2 | 1250 | 5.6 | 92 |
MC3 | 1450 | 5.9 | 96 |
Table 1 Sintering temperature, density and sample label of processed model composites.
Model composites | Sintering temperature (°C) | Density | |
---|---|---|---|
Abs (g/cm3) | Rel (%) | ||
MC1 | 1200 | 5.4 | 88 |
MC2 | 1250 | 5.6 | 92 |
MC3 | 1450 | 5.9 | 96 |
Fig. 3. (a) TEM image of a typical interface in MC3; (b) HRTEM and corresponding FFT image of SiCf/Yb2Si2O7 interface in MC3. HRTEM shows a smooth boundary between SiC and Yb2Si2O7. FFT reveals the crystallographic orientation relationship is: (111) SiC // ($\left( \bar{1}11 \right)$) Yb2Si2O7 and $\left[ 01\bar{1} \right]$ SiC // [101] Yb2Si2O7, (c) lattice fringes extent smoothly from Yb2Si2O7 to SiC, and interface misfit dislocations are plotted.
Fig. 4. Crack-interface interaction in model composites. (a) and (b) illustrate the deflection of two cracks around the fiber in MC1; (c) and (d) show the moderate crack deflection at interface in MC2; and (e) and (f) demonstrate crack penetration through the interface in MC3.
Fig. 5. Load-displacement curves of (a) MC 2, (b) MC1and (c) MC3 in fiber push out test; (d) schematics the typical stages during single fiber push out test: A-fiber surface deformation; B-initial debond at interface; C-unstable debond at maximum load, and D-fiber sliding.
Fig. 6. SEM images of pushed out fiber in MC2. (a) front side shows fiber is pushed into Yb2Si2O7; (b) back side shows the fiber is pushed out with no damage and (c) high magnification image shows extrusion of Yb2Si2O7 nearby the fiber.
Fig. 7. XRT sections of interface in MC2 after push out test. (a) section image parallel to the fiber direction. (b) radial cracks initiated at interface near the front side of indentation.
Model composites | Pd(N) | τf (MPa) | ΓRE(J/m2) | Γi/Γf | Crack-interface |
---|---|---|---|---|---|
MC1 | 0.9 ± 0.2 | 7.6 ± 1.9 | 0.4 ± 0.1 | 0.02 | Deflection |
MC2 | 2.1 ± 0.1 | 17.5 ± 2.7 | 1.8 ± 0.2 | 0.09 | Deflection |
MC3 | >5 | >50 | >9.96 | >0.49 | Penetration |
Table 2 Interfacial parameters, including initial load, sliding stress, debonding energy, Γi/Γf, and crack-fiber interaction mechanisms of the model composites.
Model composites | Pd(N) | τf (MPa) | ΓRE(J/m2) | Γi/Γf | Crack-interface |
---|---|---|---|---|---|
MC1 | 0.9 ± 0.2 | 7.6 ± 1.9 | 0.4 ± 0.1 | 0.02 | Deflection |
MC2 | 2.1 ± 0.1 | 17.5 ± 2.7 | 1.8 ± 0.2 | 0.09 | Deflection |
MC3 | >5 | >50 | >9.96 | >0.49 | Penetration |
Fig. 8. Master curve for debond adapted from Pompidou and Lamon. The SiC-fiber/Yb2Si2O7 interface demonstrates higher σic+ than SiC-matrix/Yb2Si2O7 interface.
Fig. 9. Comparison of weak and strengthened interface according to interfacial strength and sliding stress, and the corresponding mechanisms of mechanical fuse. (*: the interfacial parameters are estimated from literature.).
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