J. Mater. Sci. Technol. ›› 2020, Vol. 47: 68-75.DOI: 10.1016/j.jmst.2020.02.010
• Research Article • Previous Articles Next Articles
Yingdong Zhanga,b, Fusen Yuana,b, Fuzhou Hana,b, Muhammad Alia,b, Wenbin Guoa,b, Geping Lia,*, Chengze Liua,b, Hengfei Gua,c
Received:
2019-10-25
Revised:
2019-12-11
Accepted:
2020-01-07
Published:
2020-06-15
Online:
2020-06-24
Contact:
Geping Li
Yingdong Zhang, Fusen Yuan, Fuzhou Han, Muhammad Ali, Wenbin Guo, Geping Li, Chengze Liu, Hengfei Gu. The influence of microtexture on the formation mechanism of nodules in Zircaloy-4 alloy tube[J]. J. Mater. Sci. Technol., 2020, 47: 68-75.
Fig. 3. A schematic diagram of the relationship between the sample coordinate system and crystal coordinate system; (a) sample coordinate system. (b) the relationship between sample coordinate system and crystal coordinate system. (c) crystal coordinate system.
Fig. 4. (a, b) IPF maps of the grains in the outer and inner walls of the Zr-4 alloy tube, respectively. (b, d) the {0001}, $\{11\bar{2}0\}$ and $\{10\bar{1}0\}$ pole figures of (a, b), respectively. (e, f) the three-dimensional (3-D) model of the main crystal orientation of the outer and inner walls of the Zr-4 alloy tube, respectively.
Fig. 5. The SEM micrographs of the oxide ?lm formed on the CS of Zr-4 alloy tube after exposure to corrosion environment for 3 days (a and b) and 30 days (c and d).
Fig. 6. (a) Combination of IPF map and SEM image of grains in the CS. (b) Combination of phase map and SEM image of grains in the CS. (c) 3-D schematic diagrams of the main crystal orientation in the CS. (d) {0001}, $\{11\bar{2}0\}$ and $\{10\bar{1}0\}$ pole figures of α-Zr grains in the CS, respectively.
Fig. 8. (a, b) Combination of IPF map and SEM image of the CS in oxidized Zircaloy-4 sample; (c, d) pole figures of (a and b), respectively; (e) three-dimensional schematic diagrams of the main crystal orientation in CS; (f) three- dimensional schematic diagram of green plane perpendicular to the Y direction (yellow arrow), Y direction belongs to the sample coordinate system.
Fig. 9. (a, b) Combination of IPF map and SEM image of nodular and uniform corrosion region in the CS of the oxidized Zircaloy-4 sample, respectively; (c, d) pole figures of the grains in (a, b), respectively; (e, f) the thickness of oxide film and three-dimensional schematic diagram of grains in the nodular and uniform corrosion region, respectively.
Fig. 10. The relationship between the thickness of oxide layer and the crystal orientation in Zr-4 alloy tube. Different color and shape of the markers in the inverse pole figure denote the different grains. Two lines with different thickness are used to link the markers having a same range of oxide layer thickness.
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