J. Mater. Sci. Technol. ›› 2020, Vol. 54: 171-180.DOI: 10.1016/j.jmst.2020.02.005
• Research Article • Previous Articles Next Articles
Mei Raoa, Guoqiang Luoa,*(), Jian Zhanga, Yiyu Wangb, Qiang Shena, Lianmeng Zhanga
Received:
2019-07-18
Revised:
2019-11-12
Accepted:
2019-11-21
Published:
2020-10-01
Online:
2020-10-21
Contact:
Guoqiang Luo
Mei Rao, Guoqiang Luo, Jian Zhang, Yiyu Wang, Qiang Shen, Lianmeng Zhang. Effect of Ni content in Cu1-xNix coating on microstructure evolution and mechanical properties of W/Mo joint via low-temperature diffusion bonding[J]. J. Mater. Sci. Technol., 2020, 54: 171-180.
Materials | Elemental Composition (at.%) | |||||
---|---|---|---|---|---|---|
W | Mo | Fe | Ni | Ti | V | |
93W | Bal. | <0.02 | 3 | 4 | <0.01 | <0.01 |
Mo1 | <0.02 | Bal. | <0.02 | <0.01 | - | <0.01 |
Table 1 Chemical compositions of 93W and Mo1.
Materials | Elemental Composition (at.%) | |||||
---|---|---|---|---|---|---|
W | Mo | Fe | Ni | Ti | V | |
93W | Bal. | <0.02 | 3 | 4 | <0.01 | <0.01 |
Mo1 | <0.02 | Bal. | <0.02 | <0.01 | - | <0.01 |
Fig. 3. Interfacial morphology and elemental distributions of Cu0.75Ni0.25 coating on Mo1 alloy: (a) interfacial morphology, (b) line scanning and (c-e) area scanning of the Cu0.75Ni0.25 coating/Mo1 interface.
Fig. 7. Elemental distributions of W/Mo joint with Cu0.75Ni0.25 coating interlayer: (a) bright field TEM image of interface; (b) dark field TEM image of interface; (c-i) elemental area distributions of diffusion; (h) and (i) elemental distributions across bonded joint marked in (b).
Fig. 9. HRTEM images partially of W/Mo joint with Cu0.75Ni0.25 coating interlayer: (a-d) magnified view of area enclosed by white rectangle in Fig. 7(a).
Area | Elemental Composition (at.%) | Possible Phases | ||||
---|---|---|---|---|---|---|
W | Mo | Cu | Fe | Ni | ||
1 | 62.84 | - | 8.02 | 5.73 | 6.44 | W(ss, Cu, Ni, Fe) |
2 | - | 84.49 | 10.83 | - | 4.67 | Mo(ss, Cu, Ni) |
3 | - | - | 73.95 | 1.56 | 24.49 | Cu(ss, Ni, Fe) |
Table 2 Elemental composition of the regions marked in Fig. 12.
Area | Elemental Composition (at.%) | Possible Phases | ||||
---|---|---|---|---|---|---|
W | Mo | Cu | Fe | Ni | ||
1 | 62.84 | - | 8.02 | 5.73 | 6.44 | W(ss, Cu, Ni, Fe) |
2 | - | 84.49 | 10.83 | - | 4.67 | Mo(ss, Cu, Ni) |
3 | - | - | 73.95 | 1.56 | 24.49 | Cu(ss, Ni, Fe) |
Area | Elemental Composition (at.%) | Possible Phases | ||||
---|---|---|---|---|---|---|
W | Mo | Cu | Fe | Ni | ||
1 | - | - | 74.04 | 1.78 | 24.18 | Cu(ss, Ni, Fe) |
2 | 57.60 | - | 19.27 | 8.80 | 14.33 | W(ss, Cu, Ni, Fe) |
Table 3 Elemental composition of the regions marked in Fig. 13.
Area | Elemental Composition (at.%) | Possible Phases | ||||
---|---|---|---|---|---|---|
W | Mo | Cu | Fe | Ni | ||
1 | - | - | 74.04 | 1.78 | 24.18 | Cu(ss, Ni, Fe) |
2 | 57.60 | - | 19.27 | 8.80 | 14.33 | W(ss, Cu, Ni, Fe) |
Fig. 14. Fracture morphology and EDS analysis of W/Mo joints with Cu0.25Ni0.75 coating interlayer on 93W side: (a) SEM image; (b) amplified SEM micrograph; (c) EDS analysis of (b).
Fig. 15. Schematic diagrams of microstructure evolution and fracture of W/Mo joints with different Ni content in Cu1-xNix coating interlayer: (a) Cu and Cu0.75Ni0.25; (b) Cu0.5Ni0.5 and (c) Cu0.25Ni0.75.
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