J. Mater. Sci. Technol. ›› 2020, Vol. 47: 76-87.DOI: 10.1016/j.jmst.2020.02.004
• Research Article • Previous Articles Next Articles
Fangqiang Ninga,b, Jibo Tana, Xinqiang Wua,*()
Received:
2019-07-16
Revised:
2019-11-19
Accepted:
2019-11-25
Published:
2020-06-15
Online:
2020-06-24
Contact:
Xinqiang Wu
Fangqiang Ning, Jibo Tan, Xinqiang Wu. Effects of 405 stainless steel on crevice corrosion behavior of Alloy 690 in high-temperature pure water[J]. J. Mater. Sci. Technol., 2020, 47: 76-87.
Materials | C | N | S | P | Mn | Ti | Al | Si | Cu | Fe | Cr | Ni |
---|---|---|---|---|---|---|---|---|---|---|---|---|
Alloy 690 | 0.03 | 0.013 | 0.001 | 0.007 | 0.29 | 0.2 | 0.2 | 0.29 | 0.01 | 10.5 | 29.73 | 57.7 |
405 SS | 0.05 | - | 0.001 | 0.015 | 0.45 | 0.01 | 0.02 | 0.33 | - | 86.66 | 12.37 | 0.094 |
Table 1 Chemical compositions of Alloy 690 and 405 SS (wt.%).
Materials | C | N | S | P | Mn | Ti | Al | Si | Cu | Fe | Cr | Ni |
---|---|---|---|---|---|---|---|---|---|---|---|---|
Alloy 690 | 0.03 | 0.013 | 0.001 | 0.007 | 0.29 | 0.2 | 0.2 | 0.29 | 0.01 | 10.5 | 29.73 | 57.7 |
405 SS | 0.05 | - | 0.001 | 0.015 | 0.45 | 0.01 | 0.02 | 0.33 | - | 86.66 | 12.37 | 0.094 |
Solution | Deionized water |
---|---|
Inlet water conductivity | 0.06-0.075 μS cm-1 |
Flow rate | 9-10 L h-1 |
Pressure | 8 MPa |
Temperature in autoclave | 290 ± 2 °C |
Dissolved oxygen | 3 ppm (by weight) |
Exposure time | 500 h |
Table 2 Experimental conditions in the present work.
Solution | Deionized water |
---|---|
Inlet water conductivity | 0.06-0.075 μS cm-1 |
Flow rate | 9-10 L h-1 |
Pressure | 8 MPa |
Temperature in autoclave | 290 ± 2 °C |
Dissolved oxygen | 3 ppm (by weight) |
Exposure time | 500 h |
Fig. 2. Surface morphologies of crevice specimens after 500 h exposure test in 290 °C water containing 3 ppm DO: (a) Alloy 690; (b) 405 SS; (c) magnified image of rectangular area in (a); (d) magnified image of rectangular area in (b).
Fig. 3. XRD patterns of oxide films formed on crevice specimens after 500 h exposure test in 290 °C water containing 3 ppm DO: (a) Alloy 690, (b) 405 SS, (c, d) magnified images of rectangular areas in (a); (e, f, and g) magnified images of rectangular areas in (b).
Fig. 4. Raman spectra of oxide films formed on crevice specimens after 500 h exposure test in 290 °C water containing 3 ppm DO: (a-e) Alloy 690; (f-i) 405 SS.
Fig. 5. SEM morphologies of oxide films formed on crevice specimens after 500 h exposure test in 290 °C water containing 3 ppm DO: (a) free surface of Alloy 690; (b-d) crevice mouth of Alloy 690; (e) site within the crevice of Alloy 690; (f) deeper site within the crevice of Alloy 690; (g) crevice mouth of 405 SS; (h) site within the crevice of 405 SS; (i) deeper site within the crevice of 405 SS.
Fig. 6. XPS depth profiles of Fe (a), Ni (b), Cr (c), and O (d) in the oxide films formed on Alloy 690 after 500 h exposure test in 290 °C water containing 3 ppm DO.
Fig. 7. XPS depth profiles of O in oxide films formed on deeper sites within the crevice of Alloy 690 or 405 SS after 500 h exposure tests in 290 °C water containing 3 ppm DO.
Fig. 8. TEM observation and analysis of cross-section of oxide film formed at crevice mouth of Alloy 690 after 500 h exposure test in 290 °C water containing 3 ppm DO: (a) TEM observation of the cross-section of the oxide film; (b) mappings for Ni, Cr, Fe and O; (c) EDX point-scan collected along line shown in (a); (d) selected area electron diffraction patterns and high resolution TEM observation of oxide film.
Fig. 9. TEM observation and analysis of the cross-section of oxide film formed within the crevice of Alloy 690 after 500 h exposure tests in 290 °C water containing 3 ppm DO: (a) TEM observation of the cross-section of the oxide film; (b) mappings for Ni, Cr, Fe and O; (c) EDX point-scan collected along line shown in (a); (d) selected area electron diffraction patterns and high resolution TEM observation of oxide film.
Fig. 10. TEM observation and analysis of cross-section of oxide film formed at deeper site within the crevice of Alloy 690 after 500 h exposure tests in 290 °C water containing 3 ppm DO: (a) TEM observation of the cross-section of the oxide film; (b) mappings for Ni, Cr, Fe and O; (c) EDX point-scan collected along line shown in (a); (d) selected area electron diffraction patterns and high resolution TEM observation of oxide film.
Fig. 11. EIS results of Alloy 690 and 405 SS in 290 °C water with different DO levels: (a) Nyquist plots; (b) equivalent circuit used to simulate the EIS results.
Fig. 12. Schematics showing the influencing mechanism of 405 SS on oxidation behavior of Alloy 690 during crevice corrosion in 290 °C water containing 3 ppm DO.
[1] | S.J. Zinkle, G.S. Was, Acta Mater. 61 (2013) 735-758. |
[2] | A.J. Sedriks, J.W. Schultz, M.A. Cordovi, Corros. Eng. 28 (1979) 82-95. |
[3] | S.Y. Persaud, S. Ramamurthy, R.C. Newman, Corros. Sci. 90 (2015) 606-613. |
[4] | J. Liao, X. Wu, J. Tan, L. Tang, H. Qian, Y. Xie, Corros. Sci. 133 (2018) 423-431. |
[5] | H. Jiang, J. Xiao, Corrosion 73 (2017) 320-325. |
[6] | G.R. Engelhardt, D.D. Macdonald, P.J. Millett, Corros. Sci. 41 (1999) 2165-2190. |
[7] | G.R. Engelhardt, D.D. Macdonald, P.J. Millett, Corros. Sci. 41 (1999) 2191-2211. |
[8] | J. Abellà, I. Balachov, D.D. Macdonald, P.J. Millet, Corros. Sci. 44 (2002) 191-205. |
[9] | D. Chen, X. Wu, E.-H. Han, H. Sun, Corrosion 71 (2015) 1213-1223. |
[10] | D. Chen, E.-H. Han, X. Wu, Corros. Sci. 111 (2016) 518-530. |
[11] | B.D. Force, H. Pickering, JOM 47 (1995) 22-27. |
[12] | D.F. Taylor, Corrosion 35 (1979) 550-559. |
[13] | S.M. Sharland, Corros. Sci. 27 (1987) 289-323. |
[14] | Y.Z. Li, X.P. Guo, G.A. Zhang, Corros. Sci. 123 (2017) 228-242. |
[15] | F.M. Song, Corros. Sci. 50 (2008) 3287-3295. |
[16] | S.P. White, G.J. Weir, N.J. Laycock, Corros. Sci. 42 (2000) 605-629. |
[17] | G.F. Kennell, R.W. Evitts, K.L. Heppner, Corros. Sci. 50 (2008) 1716-1725. |
[18] | N. Satio, H. Sakamoto, K. Sugimoto, Corrosion 54 (1998) 700-712. |
[19] | T.E. Standish, M. Yari, D.W. Shoesmith, J.J. Noël. Electrochem. Soc. 164 (2017) 788-795. |
[20] | P.T. Jakobsen, E. Maahn, Corros. Sci. 43 (2001) 1693-1709. |
[21] | X. He, J.J. Noël, D.W. Shoesmith, J. Electrochem. Soc. 149 (2002) 440-449. |
[22] | Y. Sun, S. Wu, D.-H. Xia, L. Xu, J. Wang, S. Song, H. Fan, Z. Gao, J. Zhang, Z. Wu, W. Hu, Corros. Sci. 140 (2018) 260-271. |
[23] | W. Kuang, E.-H. Han, X. Wu, J. Rao, Corros. Sci. 52 (2010) 3654-3660. |
[24] | W. Kuang, X. Wu, E.-H. Han, Corros. Sci. 69 (2013) 197-204. |
[25] | W. Kuang, X. Wu, E.-H. Han, J. Rao, Corros. Sci. 53 (2011) 3853-3860. |
[26] | J.E. Maslar, W.S. Hurst, W.J. Bowers, J.H. Hendricks, E.S. Windsor, J. Electrochem. Soc. 156 (2009) C103-C113. |
[27] | J. Kim, K.J. Choi, C.B. Bahn, J.H. Kim, J. Nucl. Mater. 449 (2014) 181-187. |
[28] | X. Zhong, E.-H. Han, X.Wu, Corros. Sci. 66 (2013) 369-379. |
[29] | J.E. Maslar, W.S. Hurst, W.J. Bowers, J.H. Hendricks, M.I. Aquino, J. Electrochem. Soc. 147 (2000) 2532-2542. |
[30] | D.L. A. de Faria, S.V. Silva, M.T. de Oliveira, J. Raman Spectrosc. 28 (1997) 873-878. |
[31] | F. Ning, X. Wu, J. Tan, J. Nucl. Mater. 515 (2019) 326-337. |
[32] | Y. Han, J. Mei, Q. Peng, E.-H. Han, W.Ke, Corros. Sci. 98 (2015) 72-80. |
[33] | P. Deng, Q. Peng, E.-H. Han, W. Ke, C. Sun, Z. Jiao, Corros. Sci. 127 (2017) 91-100. |
[34] | J. Xu, T. Shoji, Corros. Sci. 104 (2016) 248-259. |
[35] | J. Xu, T. Shoji, C. Jang, Corros. Sci. 97 (2015) 115-125. |
[36] |
C. Ma, Q. Peng, J. Mei, E.-H. Han, W. Ke, J. Mater. Sci. Technol. 34 (2018) 1823-1834.
DOI URL |
[37] |
J. Wang, J. Wang, J. Mater. Sci. Technol. 31 (2015) 1039-1046.
DOI URL |
[38] | J. Wang, J. Wang, H. Ming, Z. Zhang, E.-H. Han, J.Mater. Sci. Technol. 34 (2018) 1419-1427. |
[39] | H. Sun, X. Wu, E.-H. Han, Corros.Sci. 51 (2009) 2840-2847. |
[40] |
J. Huang, X. Liu, E.-H. Han, X. Wu, Corros. Sci. 53 (2011) 3254-3261.
DOI URL |
[41] |
F.H. Sweeton, R.E. Mesmer, C.F. Baes, J. Solution Chem. 3 (1974) 191-214.
DOI URL |
[42] |
X. Ru, J. Ma, Z. Lu, J. Chen, G. Han, J. Zhang, P. Hu, X. Liang, W. Tang, J. Nucl. Mater. 509 (2018) 29-42.
DOI URL |
[43] | X. Zhong, X. Wu, E.-H. Han, J. Mater. Sci. Technol. 34 (2018) 561-569. |
[44] |
D.D. Macdonald, M.U. Macdonald, J. Electrochem. Soc. 137 (1990) 2395-2402.
DOI URL |
[45] |
D.H. Lister, R.D. Davidson, E. McAlpine, Corros. Sci. 27 (1987) 113-140.
DOI URL |
[46] |
J. Wang, X. Li, F. Huang, Z. Zhang, J. Wang, R.W. Staehle, Corrosion 70 (2014) 598-614.
DOI URL |
[47] |
W. Kuang, X. Wu, E.-H. Han, Corros. Sci. 63 (2012) 259-266.
DOI URL |
[48] |
L. Marchetti, S. Perrin, F. Jambon, M. Pijolat, Corros. Sci. 102 (2016) 24-35.
DOI URL |
[49] | D.D. Macdonald, J. Electrochem. Soc. 139 (1992) 3432-3449. |
[50] |
D.D. Macdonald, Pure Appl. Chem. 71 (1999) 951-978.
DOI URL |
[51] | B. Stellwag, Corros. Sci. 40 (1998) 337-370. |
[52] | P. Deng, Q. Peng, E.-H. Han, W. Ke, Corrosion 73 (2017) 1237-1249. |
[53] | R.J. Lemire, G.A. McRae, J. Nucl. Mater. 294 (2001) 141-147. |
[54] |
K. Kruska, S. Lozano-Perez, D.W. Saxey, T. Terachi, T. Yamada, T. Smith, D.W. George, Corros. Sci. 63 (2012) 225-233.
DOI URL |
[55] |
N.K. Das, K. Suzuki, K. Ogawa, T. Shoji, Corros. Sci. 51 (2009) 908-913.
DOI URL |
[56] |
H. Sun, X. Wu, E.-H. Han, Corros. Sci. 51 (2009) 2565-2572.
DOI URL |
[57] |
J. Robertson, Corros. Sci. 32 (1991) 443-465.
DOI URL |
[58] |
Z. Zhang, J. Wang, E.-H. Han, W. Ke, J. Mater. Sci. Technol. 30 (2014) 1181-1192.
DOI URL |
[1] | Lei Luo, Liangshun Luo, Robert O. Ritchie, Yanqing Su, Binbin Wang, Liang Wang, Ruirun Chen, Jingjie Guo, Hengzhi Fu. Optimizing the microstructures and mechanical properties of Al-Cu-based alloys with large solidification intervals by coupling travelling magnetic fields with sequential solidification [J]. J. Mater. Sci. Technol., 2021, 61(0): 100-113. |
[2] | Qianqian Jin, Xiaohong Shao, Shijian Zheng, Yangtao Zhou, Bo Zhang, Xiuliang Ma. Interfacial dislocations dominated lateral growth of long-period stacking ordered phase in Mg alloys [J]. J. Mater. Sci. Technol., 2021, 61(0): 114-118. |
[3] | Hui Jiang, Dongxu Qiao, Wenna Jiao, Kaiming Han, Yiping Lu, Peter K. Liaw. Tensile deformation behavior and mechanical properties of a bulk cast Al0.9CoFeNi2 eutectic high-entropy alloy [J]. J. Mater. Sci. Technol., 2021, 61(0): 119-124. |
[4] | Dan Zhang, Qi Han, Kun Yu, Xiaopeng Lu, Ying Liu, Ze Lu, Qiang Wang. Antibacterial activities against Porphyromonas gingivalis and biological characteristics of copper-bearing PEO coatings on magnesium [J]. J. Mater. Sci. Technol., 2021, 61(0): 33-45. |
[5] | Qin Xu, Dezhi Chen, Chongyang Tan, Xiaoqin Bi, Qi Wang, Hongzhi Cui, Shuyan Zhang, Ruirun Chen. NbMoTiVSix refractory high entropy alloys strengthened by forming BCC phase and silicide eutectic structure [J]. J. Mater. Sci. Technol., 2021, 60(0): 1-7. |
[6] | Kunming Pan, Yanping Yang, Shizhong Wei, Honghui Wu, Zhili Dong, Yuan Wu, Shuize Wang, Laiqi Zhang, Junping Lin, Xinping Mao. Oxidation behavior of Mo-Si-B alloys at medium-to-high temperatures [J]. J. Mater. Sci. Technol., 2021, 60(0): 113-127. |
[7] | Xiaoxu Liu, Yong Du, Shuhong Liu, Kaiming Cheng, Zhihong Zhang. Phase equilibria and crystal structure of ternary compounds in Al-rich corner of Al-Er-Y system at 673 and 873K [J]. J. Mater. Sci. Technol., 2021, 60(0): 128-138. |
[8] | K.J. Tan, X.G. Wang, J.J. Liang, J. Meng, Y.Z. Zhou, X.F. Sun. Effects of rejuvenation heat treatment on microstructure and creep property of a Ni-based single crystal superalloy [J]. J. Mater. Sci. Technol., 2021, 60(0): 206-215. |
[9] | Hui Xiao, Manping Cheng, Lijun Song. Direct fabrication of single-crystal-like structure using quasi-continuous-wave laser additive manufacturing [J]. J. Mater. Sci. Technol., 2021, 60(0): 216-221. |
[10] | Zijuan Xu, Zhongtao Li, Yang Tong, Weidong Zhang, Zhenggang Wu. Microstructural and mechanical behavior of a CoCrFeNiCu4 non-equiatomic high entropy alloy [J]. J. Mater. Sci. Technol., 2021, 60(0): 35-43. |
[11] | B.N. Du, Z.Y. Hu, L.Y. Sheng, D.K. Xu, Y.X. Qiao, B.J. Wang, J. Wang, Y.F. Zheng, T.F. Xi. Microstructural characteristics and mechanical properties of the hot extruded Mg-Zn-Y-Nd alloys [J]. J. Mater. Sci. Technol., 2021, 60(0): 44-55. |
[12] | Xinyue Tang, Junchao Wang, Jing Li, Xinglai Zhang, Peiqing La, Xin Jiang, Baodan Liu. In-situ growth of large-area monolithic Fe2O3/TiO2 catalysts on flexible Ti mesh for CO oxidation [J]. J. Mater. Sci. Technol., 2021, 69(0): 119-128. |
[13] | Tao Zheng, Xiaobing Hu, Feng He, Qingfeng Wu, Bin Han, Chen Da, Junjie Li, Zhijun Wang, Jincheng Wang, Ji-jung Kai, Zhenhai Xia, C.T. Liu. Tailoring nanoprecipitates for ultra-strong high-entropy alloys via machine learning and prestrain aging [J]. J. Mater. Sci. Technol., 2021, 69(0): 156-167. |
[14] | Zihong Wang, Xin Lin, Yao Tang, Nan Kang, Xuehao Gao, Shuoqing Shi, Weidong Huang. Laser-based directed energy deposition of novel Sc/Zr-modified Al-Mg alloys: columnar-to-equiaxed transition and aging hardening behavior [J]. J. Mater. Sci. Technol., 2021, 69(0): 168-179. |
[15] | Yeshun Huang, Xinguang Wang, Chuanyong Cui, Zihao Tan, Jinguo Li, Yanhong Yang, Jinlai Liu, Yizhou Zhou, Xiaofeng Sun. Effect of thermal exposure on the microstructure and creep properties of a fourth-generation Ni-based single crystal superalloy [J]. J. Mater. Sci. Technol., 2021, 69(0): 180-187. |
Viewed | ||||||
Full text |
|
|||||
Abstract |
|
|||||