J. Mater. Sci. Technol. ›› 2020, Vol. 49: 81-90.DOI: 10.1016/j.jmst.2020.01.053
• Research Article • Previous Articles Next Articles
Pablo D. Enrique*(), Ehsan Marzbanrad, Yahya Mahmoodkhani, Ali Keshavarzkermani, Hashem Al Momani, Ehsan Toyserkani, Norman Y. Zhou
Received:
2019-12-17
Revised:
2020-01-08
Accepted:
2020-01-14
Published:
2020-07-15
Online:
2020-07-17
Contact:
Pablo D. Enrique
Pablo D. Enrique, Ehsan Marzbanrad, Yahya Mahmoodkhani, Ali Keshavarzkermani, Hashem Al Momani, Ehsan Toyserkani, Norman Y. Zhou. Design of binder jet additive manufactured co-continuous ceramic-reinforced metal matrix composites[J]. J. Mater. Sci. Technol., 2020, 49: 81-90.
Fig. 2. SEM images of particles on surface of a) BJAM alloy 625, b) BJAM alloy 625 MMC, and EDX scans of the MMC surface showing c) Cr and d) Ni concentration.
Fig. 4. a) EBSD images of the cross-sectioned MMC showing a) a phase map, b) a kernel average misorientation map, and c) a crystal orientation inverse pole figure map.
Sample | Ni | Cr | Mo | Fe | Nb |
---|---|---|---|---|---|
Nominal alloy 625 | >58 | 20-23 | 8-10 | <5 | 3.15-4.15 |
Measured alloy 625 | 58.4 | 20.5 | 10.3 | 4.8 | 3.7 |
Depleted matrix | 71.2 ± 0.6 | 7.4 ± 0.3 | 7.1 ± 0.6 | 5.8 ± 0.3 | 3.1 ± 0.3 |
Hastelloy N | 71 | 7 | 16 | <4 | 0 |
Table 1 Comparison of compositions (wt%) excluding minor alloying elements.
Sample | Ni | Cr | Mo | Fe | Nb |
---|---|---|---|---|---|
Nominal alloy 625 | >58 | 20-23 | 8-10 | <5 | 3.15-4.15 |
Measured alloy 625 | 58.4 | 20.5 | 10.3 | 4.8 | 3.7 |
Depleted matrix | 71.2 ± 0.6 | 7.4 ± 0.3 | 7.1 ± 0.6 | 5.8 ± 0.3 | 3.1 ± 0.3 |
Hastelloy N | 71 | 7 | 16 | <4 | 0 |
Fig. 5. SEM images of a Cr3C2 coating on a cast alloy 625 specimen after 3 h at 1200 °C showing a) the cross section of the coating and b) the top surface of the coating, compared to SEM images of c) a particle with a Cr3C2 shell and d) a magnified view of the shell using a backscatter detector.
Temperature [°C] | k [m2 s-1] | d0 [m] | R2 |
---|---|---|---|
1100 | 6.6 × 10-16 | 0 | 0.99 |
1150 | 1.56 × 10-15 | 0 | 0.99 |
1200 | 2.38 × 10-15 | 2.72 × 10-6 | 0.99 |
Table 2 Fitted model parameters for Eq. (1) obtained from Fig. 6a.
Temperature [°C] | k [m2 s-1] | d0 [m] | R2 |
---|---|---|---|
1100 | 6.6 × 10-16 | 0 | 0.99 |
1150 | 1.56 × 10-15 | 0 | 0.99 |
1200 | 2.38 × 10-15 | 2.72 × 10-6 | 0.99 |
Fig. 6. a) Thickness of the Cr3C2 coating on cast alloy 625 as a function of time at various temperatures and b) an Arrhenius plot showing the logarithm of the growth rate constant as a function of the inverse temperature.
System | k0 [m2 s-1] | Ea [kJ mol-1] | R2 |
---|---|---|---|
This study | 1.2 × 10-7 | 216 | 0.97 |
Table 3 Fitted model parameters for Eq. (2) obtained from Fig. 6b.
System | k0 [m2 s-1] | Ea [kJ mol-1] | R2 |
---|---|---|---|
This study | 1.2 × 10-7 | 216 | 0.97 |
Fig. 7. EDX line scans of cast alloy 625 samples with zb60 coatings exposed to 1200 °C showing Cr depletion over time as a function of distance from the carbide-matrix interface.
Fig. 9. Maximum Cr3C2 shell volume fraction achievable with varying Cr concentrations in the starting powder. Values for some Ni-based alloys and the current study’s MMC are shown, with adjustments (no-fill shapes) for Mo solubility in the Cr3C2 shell.
Fig. 10. Wear profiles using ZrO2 on a) BJAM alloy 625, b) BJAM alloy 625 MMC, and using Si3N4 on c) BJAM alloy 625 and d) BJAM alloy 625 MMC. Wear tracks are shown from e) conditions in (a), and f) conditions in (b).
Pin Material | (kw1) BJAM alloy 625 | (kw2) BJAM MMC | kw1/kw2 ratio |
---|---|---|---|
ZrO2 | 4.39E-12 | 1.42E-12 | 3.09:1 |
Si3N4 | 3.70E-12 | 1.49E-12 | 2.49:1 |
Table 4 Specific wear rate (kw) in units of m2N-1.
Pin Material | (kw1) BJAM alloy 625 | (kw2) BJAM MMC | kw1/kw2 ratio |
---|---|---|---|
ZrO2 | 4.39E-12 | 1.42E-12 | 3.09:1 |
Si3N4 | 3.70E-12 | 1.49E-12 | 2.49:1 |
Fig. 12. SEM image of MMC showing a) crack propagation in the Cr3C2 phase blunted by the Ni matrix and b) plastic deformation at the Ni-Cr3C2 interface.
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