J. Mater. Sci. Technol. ›› 2017, Vol. 33 ›› Issue (5): 492-498.DOI: 10.1016/j.jmst.2016.03.016
• Orginal Article • Previous Articles Next Articles
Chen Xiaoguang1,2,*(), Xie Ruishan3, Lai Zhiwei2, Liu Lei2, Yan Jiuchun1,*(), Zou Guisheng2
Received:
2015-08-20
Revised:
2015-12-09
Accepted:
2015-12-22
Online:
2017-05-20
Published:
2017-05-17
Contact:
Chen Xiaoguang,Yan Jiuchun
About author:
These authors contributed equally to this work.
Chen Xiaoguang, Xie Ruishan, Lai Zhiwei, Liu Lei, Yan Jiuchun, Zou Guisheng. Interfacial Structure and Formation Mechanism of Ultrasonic-assisted Brazed Joint of SiC Ceramics with Al-12Si Filler Metals in Air[J]. J. Mater. Sci. Technol., 2017, 33(5): 492-498.
Fig. 4. Microstructure and fracture behavior of the joint for an ultrasonic time of 4 s: (a) whole joint; (b) interface; (c) fracture path in the joint; (d) fracture surface and the local magnification.
Fig. 6. Microstructure of the interface of the joint for an ultrasonic time of 16 s in HRTEM: (a) bright-field image and SAED patterns of phases around the interface; (b) HRTEM image of interfacial area with a partial amorphous phase; (c) HRTEM image of interfacial area with a continuous amorphous layer.
Fig. 7. XPS analysis of the surface of SiC ceramic after thermal treatment (620 °C): (a) typical XPS survey spectra; (b) XPS spectra of the Si2p core level region.
Fig. 8. Microstructure of the interface between Al-12Si and SiCox (1100 °C, 6 h) for an ultrasonic time of 8 s: (a) backscattered electron image; (b) bright-field image and local-amplification image; (c) HRTEM image and SAED patterns of interfacial amorphous layer; (d) HRTEM image and SAED patterns of interfacial reaction product.
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