J. Mater. Sci. Technol. ›› 2014, Vol. 30 ›› Issue (11): 1145-1154.DOI: 10.1016/j.jmst.2014.08.008

• Orginal Article • Previous Articles     Next Articles

Microstructural Development and Mechanical Properties of PM Ti-45Al-2Nb-2Mn-0.8 vol.%TiB2 Processed by Field Assisted Hot Pressing

R.Muñoz-Moreno1,2,*,E.M.Ruiz-Navas1,B.Srinivasarao2,J.M.Torralba1,2   

  1. 1 Department of Materials Science and Engineering,Universidad Carlos III de Madrid,Avda.Universidad 30,28911 Leganés,Madrid,Spain; 2 IMDEA Materials Institute,C/Eric Kandel 2,28906 Getafe,Madrid,Spain
  • Received:2014-03-12 Online:2014-11-20 Published:2014-12-12
  • Contact: * Corresponding author.Ph.D.; Tel.:t34 658 574 822; Fax:t34 91 5503047; E-mail address:rocio.munoz@imdea.org (R.Mu?oz-Moreno).

Abstract: A γ-TiAl intermetallic alloy,Ti-45Al-2Nb-2Mn (at.%)-0.8 vol.%TiB2,has been processed from gas atomized prealloyed powder by field assisted hot pressing (FAHP).An initial analysis of the prealloyed powder helped on the understanding of the intermetallic sintering behavior.Atomized powder consisted of α metastable phase that transformed into α2+γ equilibrium phases by thermal treating.Different powder particle microstructures were found,which influence the microstructure development of the FAHP γ-TiAl material depending on the sintering temperature.Duplex,nearly lamellar and fully lamellar microstructures were obtained at the sintering temperatures above 1000 °C.Lower consolidation temperatures,below 1000 °C,led to the formation of an Al rich phase at powder particle boundaries,which is deleterious to the mechanical properties.High compressive yield strength of 1050 MPa was observed in samples with FAHP duplex microstructures at room temperature.Whereas nearly lamellar and fully lamellar microstructures showed yield strength values of 655 and 626 MPa at room temperature and 440 and 425 MPa at 750 °C,respectively,which are superior in comparison to similar alloys processed by other techniques.These excellent properties can be explained due to the different volume fractions of the α2 and γ phases and the refinement of the PM microstructures.