Preparation and Characterization of Ni-Ferrite Coating on Carbon Steel Coupons

Abstract

Abstract: The effect of the presence of Ni in solution as Ni-EDTA complex in lithiated water at room temperature and pH 10.5 on the formation of ferrite coating on carbon steel surface was studied in an autoclave at 523 K for 12 days at different Ni concentrations with varying amounts of free EDTA. The Ni-ferrite coating was characterized by XRD, SIMS and XPS and also bulk chemical analysis by AAS and UV-visible spectrophotometer. The chemical composition of Ni-ferrite coating showed variation with depth across solution-oxide interface to oxide-metal interface. The content of Ni in the oxide coating on the surface near solution-oxide interface was found to be higher than the average Ni content estimated by analysis after descaling the coating.

Key words:

M.P.Srinivasan, Santanu Bera, S.V.Narasimhan. Preparation and Characterization of Ni-Ferrite Coating on Carbon Steel Coupons[J]. J Mater Sci Technol, 1999, 15(05): 473-477.

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Preparation and Characterization of Ni-Ferrite Coating on Carbon Steel Coupons

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