J. Mater. Sci. Technol. ›› 2019, Vol. 35 ›› Issue (2): 322-327.DOI: 10.1016/j.jmst.2018.09.058
• Orginal Article • Previous Articles Next Articles
Wei Xua, Shiqi Xiaoa, abc*(), Gang Chenabc, Chengcheng Liua, Xuanhui Quabc
Received:
2018-06-11
Revised:
2018-07-16
Accepted:
2018-08-30
Online:
2019-02-05
Published:
2018-12-21
Contact:
XinLu
About author:
These authors contributed equally to this work.
Wei Xu, Shiqi Xiao, , Gang Chen, Chengcheng Liu, Xuanhui Qu. Fabrication of commercial pure Ti by selective laser melting using hydride-dehydride titanium powders treated by ball milling[J]. J. Mater. Sci. Technol., 2019, 35(2): 322-327.
Oxygen content (wt%) | D50 (μm) | Apparent density (g/cm3) | Tap density (g/cm3) | Angle of repose (°) | Carr’s index | |
---|---|---|---|---|---|---|
raw powder | 0.35 ± 0.04 | 33.18 ± 1.12 | 1.26 ± 0.04 | 1.88 ± 0.06 | 43.33 ± 0.11 | 65.06 ± 0.13 |
2 h | 0.41 ± 0.03 | 31.65 ± 0.66 | 1.42 ± 0.05 | 1.91 ± 0.07 | 41.23 ± 0.12 | 72.06 ± 0.16 |
4 h | 0.42 ± 0.02 | 30.15 ± 0.58 | 1.64 ± 0.02 | 2.10 ± 0.04 | 40.11 ± 0.09 | 77.74 ± 0.15 |
6 h | 0.44 ± 0.04 | 28.49 ± 1.28 | 1.54 ± 0.06 | 2.03 ± 0.06 | 40.35 ± 0.15 | 75.16 ± 0.14 |
Table 1 Characteristic parameters of raw and milled powders.
Oxygen content (wt%) | D50 (μm) | Apparent density (g/cm3) | Tap density (g/cm3) | Angle of repose (°) | Carr’s index | |
---|---|---|---|---|---|---|
raw powder | 0.35 ± 0.04 | 33.18 ± 1.12 | 1.26 ± 0.04 | 1.88 ± 0.06 | 43.33 ± 0.11 | 65.06 ± 0.13 |
2 h | 0.41 ± 0.03 | 31.65 ± 0.66 | 1.42 ± 0.05 | 1.91 ± 0.07 | 41.23 ± 0.12 | 72.06 ± 0.16 |
4 h | 0.42 ± 0.02 | 30.15 ± 0.58 | 1.64 ± 0.02 | 2.10 ± 0.04 | 40.11 ± 0.09 | 77.74 ± 0.15 |
6 h | 0.44 ± 0.04 | 28.49 ± 1.28 | 1.54 ± 0.06 | 2.03 ± 0.06 | 40.35 ± 0.15 | 75.16 ± 0.14 |
Impurity | Raw Powders | Milled Powders | SLM CP-Ti parts |
---|---|---|---|
C | 0.03 ± 0.01 | 0.07 ± 0.02 | 0.08 ± 0.02 |
O | 0.28 ± 0.05 | 0.41 ± 0.03 | 0.43 ± 0.05 |
N | 0.02 ± 0.01 | 0.02 ± 0.01 | 0.03 ± 0.01 |
Fe | 0.04 ± 0.02 | 0.09 ± 0.01 | 0.10 ± 0.02 |
Table 2 Impurity levels in raw powders, milled powders and SLM-fabricated CP-Ti specimens (wt%).
Impurity | Raw Powders | Milled Powders | SLM CP-Ti parts |
---|---|---|---|
C | 0.03 ± 0.01 | 0.07 ± 0.02 | 0.08 ± 0.02 |
O | 0.28 ± 0.05 | 0.41 ± 0.03 | 0.43 ± 0.05 |
N | 0.02 ± 0.01 | 0.02 ± 0.01 | 0.03 ± 0.01 |
Fe | 0.04 ± 0.02 | 0.09 ± 0.01 | 0.10 ± 0.02 |
Fig. 5. (a): Tensile stress-strain curves of SLM-fabricated CP-Ti, cast CP-Ti and Ti-6Al-4V; (b) comparison of SLM-fabricated CP-Ti using HDH powders, as-cast CP-Ti and Ti-6Al-4V, SLM-fabricated CP-Ti and Ti-6Al-4V from spherical powders, ASTM standard for CP-Ti and Ti-6Al-4V, SLM-fabricated Ti-Ta, and SLM-fabricated Ti-24Nb-4Zr-8Sn.
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