J. Mater. Sci. Technol. ›› 2018, Vol. 34 ›› Issue (2): 277-283.DOI: 10.1016/j.jmst.2017.11.022

Special Issue: 2017-2018年Mg合金专题 High Strength Alloys-2018

• Orginal Article • Previous Articles     Next Articles

Influence of size and distribution of W phase on strength and ductility of high strength Mg-5.1Zn-3.2Y-0.4Zr-0.4Ca alloy processed by indirect extrusion

Hansi Jianga, Xiaoguang Qiaoa, Chao Xub, Shigeharu Kamadob, Kun Wua, Mingyi Zhenga()   

  1. aSchool of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001, China
    bDepartment of Mechanical Engineering, Nagaoka University of Technology, Nagaoka 940-2188, Japan
  • Received:2017-08-05 Revised:2017-08-18 Accepted:2017-11-03 Online:2018-02-10 Published:2018-02-10

Abstract:

A high strength Mg-5.1Zn-3.2Y-0.4Zr-0.4Ca (wt%) alloy containing W phase (Mg3Y2Zn3) prepared by permanent mold direct-chill casting is indirectly extruded at 350 °C and 400 °C, respectively. The extruded alloys show bimodal grain structure consisting of fine dynamic recrystallized (DRXed) grains and unrecrystallized coarse regions containing fine W phase and β2? precipitates. The fragmented W phase particles induced by extrusion stimulate nucleation of DRXed grains, leading to the formation of fine DRXed grains, which are mainly distributed near the W particle bands along the extrusion direction. The alloy extruded at 350 °C exhibits yield strength of 373 MPa, ultimate tensile strength of 403 MPa and elongation to failure of 5.1%. While the alloy extruded at 400 °C shows lower yield strength of 332 MPa, ultimate tensile strength of 352 MPa and higher elongation to failure of 12%. The mechanical properties of the as-extruded alloys vary with the distribution and size of W phase. A higher fraction of DRXed grains is obtained due to the homogeneous distribution of micron-scale broken W phase particles in the alloy extruded at 400 °C, which can lead to higher ductility. In addition, the nano-scale dynamic W phase precipitates distributed in the unDRXed regions are refined at lower extrusion temperature. The smaller size of nano-scale W phase precipitates leads to a higher fraction of unDRXed regions which contributes to higher strength of the alloy extruded at 350 °C.

Key words: Mg alloy, Extrusion temperature, Mechanical properties, W phase, Dynamic precipitation, Bimodal structure